http://gisaxs.com/index.php?title=GISAXS_sample_requirements&feed=atom&action=historyGISAXS sample requirements - Revision history2024-03-28T16:41:08ZRevision history for this page on the wikiMediaWiki 1.31.7http://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=5897&oldid=prevKevinYager at 12:01, 3 July 20182018-07-03T12:01:26Z<p></p>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>The following gives some rough guidelines for the kinds of samples suitable for [[GISAXS]]/[[GIWAXS]] measurements. In general, GISAXS is intended to measure thin films cast on flat substrates.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>The following gives some rough guidelines for the kinds of samples suitable for [[GISAXS]]/[[GIWAXS]] measurements. In general, GISAXS is intended to measure thin films cast on flat substrates.</div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div><ins style="font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div><ins style="font-weight: bold; text-decoration: none;">Commercial silicon wafers are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield good data, as well as other common substrates (e.g. ITO). Samples are typically diced to be 1 cm by 1 cm, but samples can be bigger (up to a few inches in size) or smaller (a few mm in size). </ins></div></td></tr>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=2364&oldid=prev130.199.3.165: /* Summary */2014-09-23T00:42:42Z<p><span dir="auto"><span class="autocomment">Summary</span></span></p>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[Material:Silicon|silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. ITO).</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[Material:Silicon|silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. <ins class="diffchange diffchange-inline">[[Material:</ins>ITO<ins class="diffchange diffchange-inline">|ITO]]</ins>).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
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</table>130.199.3.165http://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=1734&oldid=prevKevinYager: /* Material */2014-09-08T15:17:04Z<p><span dir="auto"><span class="autocomment">Material</span></span></p>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Note that nominally flat substrates (e.g. silicon wafers) can become bent due to processing conditions. E.g. the stress of a spin-coater can kink a wafer.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Note that nominally flat substrates (e.g. silicon wafers) can become bent due to processing conditions. E.g. the stress of a spin-coater can kink a wafer.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Material====</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Material====</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>In principle, any substrate material can be used. There are advantages to having a substrate material that has a larger critical angle than the film being studied:</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>In principle, any substrate <ins class="diffchange diffchange-inline">[[materials|</ins>material<ins class="diffchange diffchange-inline">]] </ins>can be used. There are advantages to having a substrate material that has a larger critical angle than the film being studied:</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div># In [[reflectivity]], the region between the two critical angles will generate pseudo-waveguide modes, and provides a sensitive measure of film properties (e.g. [[absorption]]).</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div># In [[reflectivity]], the region between the two critical angles will generate pseudo-waveguide modes, and provides a sensitive measure of film properties (e.g. [[absorption]]).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div># In GISAXS, one can similarly take advantage of waveguide-like modes and intensity enhancements due to the strong reflection from the substrate.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div># In GISAXS, one can similarly take advantage of waveguide-like modes and intensity enhancements due to the strong reflection from the substrate.</div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div><ins style="font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Substrate thickness====</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Substrate thickness====</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Substrate thickness does not have any impact on GISAXS measurements. Thicker substrates can be advantageous in terms of maintaining rigorous substrate flatness (especially relevant for [[reflectivity]]); but even regular (0.5 mm thick) Si wafers are typically fine.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Substrate thickness does not have any impact on GISAXS measurements. Thicker substrates can be advantageous in terms of maintaining rigorous substrate flatness (especially relevant for [[reflectivity]]); but even regular (0.5 mm thick) Si wafers are typically fine.</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=657&oldid=prev66.249.83.102: /* Film Thickness */2014-06-14T19:53:45Z<p><span dir="auto"><span class="autocomment">Film Thickness</span></span></p>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Thin films From monolayers to microns can in principle be studied. Ideal film thickness is ~50 nm to ~300 nm; but ultimately it is the scientifically relevant thickness that should be targeted. Ultrathin layers will of course have lower total scattering intensity (and thus may <del class="diffchange diffchange-inline">necessity </del>longer exposure times). Very thick (e.g. micron) layers can be studied with GISAXS, although the large roughness typical of such films will make some kinds of measurements impossible. In particular, the film will lack a well-defined [[critical angle]], which makes the usual above/below critical measurements impossible (and of course [[x-ray waveguiding]] will also not be possible).</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Thin films From monolayers to microns can in principle be studied. Ideal film thickness is ~50 nm to ~300 nm; but ultimately it is the scientifically relevant thickness that should be targeted. Ultrathin layers will of course have lower total scattering intensity (and thus may <ins class="diffchange diffchange-inline">require </ins>longer exposure times). Very thick (e.g. micron) layers can be studied with GISAXS, although the large roughness typical of such films will make some kinds of measurements impossible. In particular, the film will lack a well-defined [[critical angle]], which makes the usual above/below critical measurements impossible (and of course [[x-ray waveguiding]] will also not be possible).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Substrate===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Substrate===</div></td></tr>
</table>66.249.83.102http://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=656&oldid=prev66.249.83.102: /* Film Thickness */2014-06-14T19:51:08Z<p><span dir="auto"><span class="autocomment">Film Thickness</span></span></p>
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<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Film Thickness===</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Thin films From monolayers to microns can in principle be studied. Ideal film thickness is ~50 nm to ~300 nm; but ultimately is <del class="diffchange diffchange-inline">it </del>the scientifically relevant thickness that should be targeted. Ultrathin layers will of course have lower total scattering intensity (and thus may necessity longer exposure times). Very thick (e.g. micron) layers can be studied with GISAXS, although the large roughness typical of such films will make some kinds of measurements impossible. In particular, the film will lack a well-defined [[critical angle]], which makes the usual above/below critical measurements impossible (and of course [[x-ray waveguiding]] will also not be possible).</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Thin films From monolayers to microns can in principle be studied. Ideal film thickness is ~50 nm to ~300 nm; but ultimately <ins class="diffchange diffchange-inline">it </ins>is the scientifically relevant thickness that should be targeted. Ultrathin layers will of course have lower total scattering intensity (and thus may necessity longer exposure times). Very thick (e.g. micron) layers can be studied with GISAXS, although the large roughness typical of such films will make some kinds of measurements impossible. In particular, the film will lack a well-defined [[critical angle]], which makes the usual above/below critical measurements impossible (and of course [[x-ray waveguiding]] will also not be possible).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Substrate===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Substrate===</div></td></tr>
</table>66.249.83.102http://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=638&oldid=prevKevinYager: /* Dimensions */2014-06-14T15:32:48Z<p><span dir="auto"><span class="autocomment">Dimensions</span></span></p>
<table class="diff diff-contentalign-left" data-mw="interface">
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<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">← Older revision</td>
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">Revision as of 15:32, 14 June 2014</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l29" >Line 29:</td>
<td colspan="2" class="diff-lineno">Line 29:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>A GISAXS beam is typically ~100 μm wide by ~50 μm tall. Because of the shallow grazing-incidence angle, the small beam height is nevertheless projected into a large stripe; usually 1-12 mm long. As such, a stretched rectangle (microns wide by mm long) of the sample surface will be probed. In principle, samples as small as 0.5 mm × 0.5 mm can be measured (with a corresponding decrease in total scattering). On the other hand, samples as large as many inches can typically be accommodated. The ideal sample size is ~10 mm × ~10 mm. This size captures most of the x-ray beam, and makes alignment relatively simple and robust.</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>A GISAXS beam is typically ~100 μm wide by ~50 μm tall. Because of the shallow grazing-incidence angle, the small beam height is nevertheless <ins class="diffchange diffchange-inline">[[beam projection|</ins>projected<ins class="diffchange diffchange-inline">]] </ins>into a large stripe; usually 1-12 mm long. As such, a stretched rectangle (microns wide by mm long) of the sample surface will be probed. In principle, samples as small as 0.5 mm × 0.5 mm can be measured (with a corresponding decrease in total scattering). On the other hand, samples as large as many inches can typically be accommodated. The ideal sample size is ~10 mm × ~10 mm. This size captures most of the x-ray beam, and makes alignment relatively simple and robust.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Edge effects===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Edge effects===</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=552&oldid=prevKevinYager: /* Structure */2014-06-11T19:00:17Z<p><span dir="auto"><span class="autocomment">Structure</span></span></p>
<table class="diff diff-contentalign-left" data-mw="interface">
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<col class="diff-content" />
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<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">← Older revision</td>
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">Revision as of 19:00, 11 June 2014</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l37" >Line 37:</td>
<td colspan="2" class="diff-lineno">Line 37:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Structure===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Structure===</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Lastly, but most importantly, the sample must have some '''structure to be probed'''. A smooth and homogeneous film without any structure will not yield any scattering signal (other than an oscillation of specular intensity arising from the film thickness). A disordered film without any well-defined structure will yield [[diffuse scattering]], but nothing else. GISAXS is thus targeted at films that have well-defined nanostructure. (GIWAXS is targeted at films with well-defined molecular-scale structure.)</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Lastly, but most importantly, the sample must have some '''structure to be probed'''. A smooth and homogeneous film without any structure will not yield any scattering signal (other than an oscillation of specular intensity arising from the film thickness). A disordered film without any well-defined structure will yield [[diffuse scattering]], but nothing else. <ins class="diffchange diffchange-inline">[[</ins>GISAXS<ins class="diffchange diffchange-inline">]] </ins>is thus targeted at films that have well-defined nanostructure. (<ins class="diffchange diffchange-inline">[[</ins>GIWAXS<ins class="diffchange diffchange-inline">]] </ins>is targeted at films with well-defined molecular-scale structure.)</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=551&oldid=prevKevinYager: /* Dimensions */2014-06-11T18:59:39Z<p><span dir="auto"><span class="autocomment">Dimensions</span></span></p>
<table class="diff diff-contentalign-left" data-mw="interface">
<col class="diff-marker" />
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<col class="diff-marker" />
<col class="diff-content" />
<tr class="diff-title" lang="en">
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">← Older revision</td>
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">Revision as of 18:59, 11 June 2014</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l29" >Line 29:</td>
<td colspan="2" class="diff-lineno">Line 29:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>A GISAXS beam is typically ~100 μm wide by ~50 μm tall. Because of the shallow grazing-incidence angle, the small beam height is nevertheless projected into a large stripe; usually 1-12 mm long. As such, a stretched rectangle (microns wide by mm long) of the sample surface will be probed. In principle, samples as small as 0.5 mm × 0.5 mm can be measured (with a corresponding decrease in total scattering). On the other hand, samples as large as many inches can typically be <del class="diffchange diffchange-inline">accomodated</del>. The <del class="diffchange diffchange-inline">idea </del>sample size is ~10 mm × ~10 mm. This size captures most of the x-ray beam, and makes alignment relatively simple and robust.</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>A GISAXS beam is typically ~100 μm wide by ~50 μm tall. Because of the shallow grazing-incidence angle, the small beam height is nevertheless projected into a large stripe; usually 1-12 mm long. As such, a stretched rectangle (microns wide by mm long) of the sample surface will be probed. In principle, samples as small as 0.5 mm × 0.5 mm can be measured (with a corresponding decrease in total scattering). On the other hand, samples as large as many inches can typically be <ins class="diffchange diffchange-inline">accommodated</ins>. The <ins class="diffchange diffchange-inline">ideal </ins>sample size is ~10 mm × ~10 mm. This size captures most of the x-ray beam, and makes alignment relatively simple and robust.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Edge effects===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Edge effects===</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=431&oldid=prevKevinYager: /* Summary */2014-06-06T18:11:23Z<p><span dir="auto"><span class="autocomment">Summary</span></span></p>
<table class="diff diff-contentalign-left" data-mw="interface">
<col class="diff-marker" />
<col class="diff-content" />
<col class="diff-marker" />
<col class="diff-content" />
<tr class="diff-title" lang="en">
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">← Older revision</td>
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">Revision as of 18:11, 6 June 2014</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l26" >Line 26:</td>
<td colspan="2" class="diff-lineno">Line 26:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[Material:|silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. ITO).</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[Material:<ins class="diffchange diffchange-inline">Silicon</ins>|silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. ITO).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td></tr>
</table>KevinYagerhttp://gisaxs.com/index.php?title=GISAXS_sample_requirements&diff=430&oldid=prevKevinYager: /* Summary */2014-06-06T18:11:10Z<p><span dir="auto"><span class="autocomment">Summary</span></span></p>
<table class="diff diff-contentalign-left" data-mw="interface">
<col class="diff-marker" />
<col class="diff-content" />
<col class="diff-marker" />
<col class="diff-content" />
<tr class="diff-title" lang="en">
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">← Older revision</td>
<td colspan="2" style="background-color: #fff; color: #222; text-align: center;">Revision as of 18:11, 6 June 2014</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l26" >Line 26:</td>
<td colspan="2" class="diff-lineno">Line 26:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>Generally, the thin film of interest is the outermost layer for GISAXS measurements. It is, however, possible to probe buried layers. Note, however, that one must consider the critical angles, and [[absorption lengths]] of layers placed on top of the film of interest. If the top layers are too thick/absorptive, then no signal will be measured. And, of course, to probe a buried layer one must be above the critical angle of all the superposed layers.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>====Summary====</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. ITO).</div></td><td class='diff-marker'>+</td><td style="color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>Despite these guidelines, in reality a wide variety of substrates are suitable. In practice, commercial single-crystal '''[[<ins class="diffchange diffchange-inline">Material:|</ins>silicon]] wafers''' are an ideal substrate choice, as they are cheap, smooth, flat, and have well-defined surface chemistry. However even glass microscope slides will yield reasonable data, as well as other common substrates (e.g. ITO).</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td><td class='diff-marker'> </td><td style="background-color: #f8f9fa; color: #222; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><div>===Dimensions===</div></td></tr>
</table>KevinYager