Difference between revisions of "GIWAXS"

From GISAXS
Jump to: navigation, search
Line 1: Line 1:
'''Grazing-Incidence Wide-Angle X-ray Scattering''' ('''GIWAXS''') is a structural measurement technique wherein wide-angle [[scattering]] is collected; i.e. large values of the [[momentum transfer]]. Because of the [[Fourier transform|inverse nature]] of [[reciprocal-space]], these large values of ''q'' [[Q value|correspond]] to small distances; WAXS generically probes molecular length-scales.
+
'''Grazing-Incidence Wide-Angle X-ray Scattering''' ('''GIWAXS''') is a structural measurement technique wherein wide-angle [[scattering]] is collected; i.e. large values of the [[momentum transfer]]. Because of the [[Fourier transform|inverse nature]] of [[reciprocal-space]], these large values of ''q'' [[Q value|correspond]] to small distances; [[WAXS]] generically probes molecular length-scales.
  
There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or ''q''-values from 0.1 Å<sup>−1</sup> to 5 Å<sup>−1</sup> (6 nm to Angstroms).
+
There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or ''q''-values from 0.1 Å<sup>−1</sup> to 5 Å<sup>−1</sup> ([[realspace]] distances from 6 nm to Angstroms).
  
 
==Example Data==
 
==Example Data==
Line 19: Line 19:
 
* A thin film of rubrene:
 
* A thin film of rubrene:
 
[[Image:Rubrene GIWAXS example.png|300px]]
 
[[Image:Rubrene GIWAXS example.png|300px]]
 
 
  
  
 
==See Also==
 
==See Also==
 
* [[GISAXS]]
 
* [[GISAXS]]

Revision as of 17:12, 14 October 2014

Grazing-Incidence Wide-Angle X-ray Scattering (GIWAXS) is a structural measurement technique wherein wide-angle scattering is collected; i.e. large values of the momentum transfer. Because of the inverse nature of reciprocal-space, these large values of q correspond to small distances; WAXS generically probes molecular length-scales.

There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or q-values from 0.1 Å−1 to 5 Å−1 (realspace distances from 6 nm to Angstroms).

Example Data

  • Different representations of data from a P3HT thin film
Raw detector image.
Data converted to q-space.
Data converted to q-space, taking into account the Ewald sphere (notice the 'missing wedge' near the qz axis).
  • A Tungsten-Nickel alloy:

TungstenNickel.png

  • A thin film of rubrene:

Rubrene GIWAXS example.png


See Also