Difference between revisions of "Refraction distortion"
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==Refraction Correction== | ==Refraction Correction== | ||
| + | The GISAXS refraction distortion shifts the data along <math>\scriptstyle q_z</math>, leaving <math>\scriptstyle q_x</math> unaffected. | ||
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* Byeongdu Lee, Insun Park, Jinhwan Yoon, Soojin Park, Jehan Kim, Kwang-Woo Kim, Taihyun Chang, and Moonhor Ree [http://pubs.acs.org/doi/abs/10.1021/ma047562d Structural Analysis of Block Copolymer Thin Films with Grazing Incidence Small-Angle X-ray Scattering] ''Macromolecules'' '''2005''', 38 (10), 4311-4323. [http://dx.doi.org/10.1021/ma047562d doi: 10.1021/ma047562d] | * Byeongdu Lee, Insun Park, Jinhwan Yoon, Soojin Park, Jehan Kim, Kwang-Woo Kim, Taihyun Chang, and Moonhor Ree [http://pubs.acs.org/doi/abs/10.1021/ma047562d Structural Analysis of Block Copolymer Thin Films with Grazing Incidence Small-Angle X-ray Scattering] ''Macromolecules'' '''2005''', 38 (10), 4311-4323. [http://dx.doi.org/10.1021/ma047562d doi: 10.1021/ma047562d] | ||
* P. Busch, M. Rauscher, D.-M. Smilgies, D. Posselt and C. M. Papadakis [http://scripts.iucr.org/cgi-bin/paper?S0021889806012337 Grazing-incidence small-angle X-ray scattering from thin polymer films with lamellar structures - the scattering cross section in the distorted-wave Born approximation] ''J. Appl. Cryst.'' '''2006''', 39, 433-442. [http://dx.doi.org/10.1107/S0021889806012337 doi: 10.1107/S0021889806012337] | * P. Busch, M. Rauscher, D.-M. Smilgies, D. Posselt and C. M. Papadakis [http://scripts.iucr.org/cgi-bin/paper?S0021889806012337 Grazing-incidence small-angle X-ray scattering from thin polymer films with lamellar structures - the scattering cross section in the distorted-wave Born approximation] ''J. Appl. Cryst.'' '''2006''', 39, 433-442. [http://dx.doi.org/10.1107/S0021889806012337 doi: 10.1107/S0021889806012337] | ||
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* D. W. Breiby, O. Bunk, J. W. Andreasen, H. T. Lemke and M. M. Nielsen [http://scripts.iucr.org/cgi-bin/paper?S0021889808001064 Simulating X-ray diffraction of textured films] ''J. Appl. Cryst.'' 2008, 41, 262-271. [http://dx.doi.org/10.1107/S0021889808001064 doi: 10.1107/S0021889808001064] | * D. W. Breiby, O. Bunk, J. W. Andreasen, H. T. Lemke and M. M. Nielsen [http://scripts.iucr.org/cgi-bin/paper?S0021889808001064 Simulating X-ray diffraction of textured films] ''J. Appl. Cryst.'' 2008, 41, 262-271. [http://dx.doi.org/10.1107/S0021889808001064 doi: 10.1107/S0021889808001064] | ||
* Lu, X.; [[Yager, K.G.]]; Johnston, D.; Black, C.T.; Ocko, B.M. '''[http://scripts.iucr.org/cgi-bin/paper?S0021889812047887 Grazing-incidence transmission X-ray scattering: surface scattering in the Born approximation]''' ''Journal of Applied Crystallography'' '''2013''', 46, 165–172. [http://dx.doi.org/10.1107/S0021889812047887 doi: 10.1107/S0021889812047887] | * Lu, X.; [[Yager, K.G.]]; Johnston, D.; Black, C.T.; Ocko, B.M. '''[http://scripts.iucr.org/cgi-bin/paper?S0021889812047887 Grazing-incidence transmission X-ray scattering: surface scattering in the Born approximation]''' ''Journal of Applied Crystallography'' '''2013''', 46, 165–172. [http://dx.doi.org/10.1107/S0021889812047887 doi: 10.1107/S0021889812047887] | ||
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==See Also== | ==See Also== | ||
Revision as of 14:05, 4 November 2015
In GISAXS, GIWAXS, and other grazing-incidence techniques, the refractive index difference between the film and the ambient causes the incident and scattered x-ray beams to be refracted. This extent of refraction depends on the incident and exit angles. Thus, the data that appears on an area detector in a grazing-incidence experiment is non-linearly distorted. This makes data interpretation more problematic.
Refraction Correction
The GISAXS refraction distortion shifts the data along , leaving unaffected.
- Byeongdu Lee, Insun Park, Jinhwan Yoon, Soojin Park, Jehan Kim, Kwang-Woo Kim, Taihyun Chang, and Moonhor Ree Structural Analysis of Block Copolymer Thin Films with Grazing Incidence Small-Angle X-ray Scattering Macromolecules 2005, 38 (10), 4311-4323. doi: 10.1021/ma047562d
- P. Busch, M. Rauscher, D.-M. Smilgies, D. Posselt and C. M. Papadakis Grazing-incidence small-angle X-ray scattering from thin polymer films with lamellar structures - the scattering cross section in the distorted-wave Born approximation J. Appl. Cryst. 2006, 39, 433-442. doi: 10.1107/S0021889806012337
- Rémi Lazzari, Frédéric Leroy, and Gilles Renaud Grazing-incidence small-angle x-ray scattering from dense packing of islands on surfaces: Development of distorted wave Born approximation and correlation between particle sizes and spacing Phys. Rev. B 2007, 76, 125411. doi: 10.1103/PhysRevB.76.125411
- D. W. Breiby, O. Bunk, J. W. Andreasen, H. T. Lemke and M. M. Nielsen Simulating X-ray diffraction of textured films J. Appl. Cryst. 2008, 41, 262-271. doi: 10.1107/S0021889808001064
- Lu, X.; Yager, K.G.; Johnston, D.; Black, C.T.; Ocko, B.M. Grazing-incidence transmission X-ray scattering: surface scattering in the Born approximation Journal of Applied Crystallography 2013, 46, 165–172. doi: 10.1107/S0021889812047887
See Also
- DWBA
- Simulating X-ray diffraction of textured films D. W. Breiby, O. Bunk, J. W. Andreasen, H. T. Lemke and M. M. Nielsen J. Appl. Cryst. 2008, 41, 262-271. doi: 10.1107/S0021889808001064
- Indexation scheme for oriented molecular thin films studied with grazing-incidence reciprocal-space mapping D.-M. Smilgies and D. R. Blasini J. Appl. Cryst. 2007, 40, 716-718. doi: 10.1107/S0021889807023382
- Grazing-incidence small-angle X-ray scattering from thin polymer films with lamellar structures - the scattering cross section in the distorted-wave Born approximation P. Busch, M. Rauscher, D.-M. Smilgies, D. Posselt and C. M. Papadakis J. Appl. Cryst. 2006, 39, 433-442. doi: 10.1107/S0021889806012337
