Difference between revisions of "GIWAXS"

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There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or ''q''-values from 0.1 Å<sup>−1</sup> to 5 Å<sup>−1</sup> (6 nm to Angstroms).
 
There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or ''q''-values from 0.1 Å<sup>−1</sup> to 5 Å<sup>−1</sup> (6 nm to Angstroms).
  
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==Example Data==
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* Different representations of data from a [[P3HT]] thin film
 
{|
 
{|
Example GIWAXS data for a [[P3HT]] thin film.
 
 
|-
 
|-
 
| [[Image:P3ht calibration01.png|thumb|200px|Raw detector image.]]
 
| [[Image:P3ht calibration01.png|thumb|200px|Raw detector image.]]
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| [[Image:P3ht calibration03.png|thumb|200px|Data converted to ''q''-space, taking into account the [[Ewald sphere]] (notice the '[[GI missing wedge|missing wedge]]' near the [[specular axis|q<sub>z</sub> axis]]).]]
 
| [[Image:P3ht calibration03.png|thumb|200px|Data converted to ''q''-space, taking into account the [[Ewald sphere]] (notice the '[[GI missing wedge|missing wedge]]' near the [[specular axis|q<sub>z</sub> axis]]).]]
 
|}
 
|}
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* A Tungsten-Nickel alloy:
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[[Image:TungstenNickel.png|300px]]
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* A thin film of rubrene:
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[[Image:Rubrene GIWAXS example.png|300px]]
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==See Also==
 
==See Also==
 
* [[GISAXS]]
 
* [[GISAXS]]

Revision as of 16:12, 14 October 2014

Grazing-Incidence Wide-Angle X-ray Scattering (GIWAXS) is a structural measurement technique wherein wide-angle scattering is collected; i.e. large values of the momentum transfer. Because of the inverse nature of reciprocal-space, these large values of q correspond to small distances; WAXS generically probes molecular length-scales.

There is no unambiguous delineation between WAXS and SAXS; generally speaking, WAXS corresponds to angles from approximately 1° to 45°, or q-values from 0.1 Å−1 to 5 Å−1 (6 nm to Angstroms).

Example Data

  • Different representations of data from a P3HT thin film
Raw detector image.
Data converted to q-space.
Data converted to q-space, taking into account the Ewald sphere (notice the 'missing wedge' near the qz axis).
  • A Tungsten-Nickel alloy:

TungstenNickel.png

  • A thin film of rubrene:

Rubrene GIWAXS example.png



See Also